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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Characterization of Materials through High Resolution Coherent Imaging
Presentation Title Simultaneous Reciprocal and Real Space X-Ray Imaging for Hierarchical Characterization of 3D Nano-Architected Metamaterials
Author(s) Matias Kagias, Seola Lee, Dula Parkinson, Nicholas W. Phillips, Julia R. Greer
On-Site Speaker (Planned) Matias Kagias
Abstract Scope The advent of 3D nanofabrication methods has given rise to a new class of materials termed nano-architected metamaterials. With their tailored 3D architecture these materials achieve unique macroscopic properties, ranging from extreme mechanical resilience to negative refractive indices. With the recent introduction of scalable 3D nanofabrication reaching sample sizes in the centimeter scale, characterizing nano-architected metamaterials poses a challenging hierarchical characterization problem. Here we present recent progress in characterizing the sub-micrometer structure of lithographically produced 3D nano-architected polymer based sheets with approximately 500 nm features and 30 micrometer thickness by combining reciprocal space and full field imaging at synchrotron sources. We utilize a two dimensional array of 3234 zone plates that allows to locally sense reciprocal information during full field imaging operation. Our experimental results demonstrate the high sensitivity of the approach for probing structural uniformity that is linked to the local elastic modulus of the imaged materials.
Proceedings Inclusion? Planned:
Keywords Characterization, Mechanical Properties, Polymers

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

AI-Driven Workflow for Autonomous High-Resolution Scanning X-Ray Microscopy
Bragg Coherent Diffractive Imaging With Twisted X-Rays
Characterization of Crystalline Materials at the Atomic Scale with X-Ray Bragg Coherent Diffraction Imaging
Coherent x-Ray Diffraction Imaging Dedicated Beamlines at PLS-II and Korea-4GSR
Direct Reciprocal Space Detection of Microelectronic Defects Using Coherent X-Ray Diffraction and Unsupervised Machine Learning
Enhanced Mineral Characterization With 3D X-Ray CT and AI-Driven Imaging
Explanation of the High-Dielectric Constant of BaTiO3 Used in Multilayer Capacitors
High-Resolution X-Ray Imaging of Integrated Circuits
High Bandwidth Scanning X-Ray Microscopy
In-Situ/Operando Bragg Coherent X-Ray Diffraction Imaging for Catalysis Studies
ML-Guided Non-Destructive 3D Metrology of Functioning Devices With an X-Ray Laser
Nanoholotomography With Coded Apertures for Efficient Dynamic Imaging of Nanomaterials
Operando and Linear Dichroic Ptychographic Spectro-Tomography of Heterogenous Catalysts
Origin of Structural Degradation in Layered Oxide Cathode for Li-Ion Batteries
Physics-Informed Self-Supervised Learning of Structural Morphology Imaged by Scanning X-Ray Diffraction Microscopy
Probing Cryogenic Strain Evolution in SrTiO3 Using Multi-Reflection Bragg Coherent Diffraction Imaging
Rapid Reconstruction of the Full Strain Tensor via Coupled Phase Retrieval With Multipeak Bragg Coherent Diffraction Imaging
Real-Time Imaging of Subsurface Dislocation Dynamics
Simultaneous Reciprocal and Real Space X-Ray Imaging for Hierarchical Characterization of 3D Nano-Architected Metamaterials
Single-Exposure Elemental Differentiation and Texture-Sensitive Phase-Retrieval Imaging with a Neutron-Counting Microchannel-Plate Detector
Single-Shot X-Ray Imaging of Density in Laser Shocked Materials for Fusion Energy Studies
Synchrotron Ptychographic X-Ray Computed Tomography (PXCT) to Study Micro-Fabricated Fully Hybrid 3D Metal-Ceramic Metamaterials
Three-Dimensional Hard X-Ray Ptychographic Reflectometry Imaging on Extended Mesoscopic Surface Structures

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