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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Mechanical Response of Materials Investigated Through Novel In-Situ Experiments and Modeling
Presentation Title Microstructural impact on brittle fracture path investigated via high-energy synchrotron techniques
Author(s) Sara Gorske, Mythreyi Ramesh, Jun-Sang Park, Peter Kenesei, Hemant Sharma, Jonathan Almer, Peter Voorhees, Katherine Faber
On-Site Speaker (Planned) Sara Gorske
Abstract Scope Brittle fracture is a difficult failure mechanism to investigate in real-time, as the speed and catastrophic nature of a growing crack front hinder many in-situ techniques. However, the double-cleavage drilled compression sample geometry allows for controlled crack growth in a ceramic material. The high X-ray energy and 360-degree rotation capability of synchrotrons provide an ideal way to investigate how a growing crack interacts with the local microstructure at many different load steps. The techniques considered are micro-computed X-ray tomography to investigate the shape and extension of the crack front, and high-energy diffraction microscopy to track the location, orientation, and average strain field of nearby grains. We present results from performing this analysis on aluminum oxynitride samples, with insight into how the size, location, and orientation of grains affect the strain distribution and how the local stresses in turn impact or impede the direction and extension length of the crack.
Proceedings Inclusion? Planned:
Keywords Ceramics, Mechanical Properties,

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Automated DIC-based local identification of various nanoscale plastic deformation mechanisms in HCP
Billion-cycle fatigue endurance enabled via grain boundary stabilization
Characterizing Phenomena in Metals and Alloys at the Single Defect Level
Contribution of slip, twinning and de-twinning to the mechanical deformation of Haynes 244® alloy at 23ºC and 650ºC
CRSS determination in α-Ti: Modelling and in-situ TEM study
Crystal Plasticity Experiments with Microstructure Clones
Data acquisition and modeling to enable microstructure tailorability in Wire Arc Additive Manufacturing
Discrete Dislocation Dynamic Simulation of Shock-Induced Plasticity in Aluminum motivated by Atomistic Data
Evaluating phase-field simulations of brittle fracture in polycrystalline materials
Evaluation of the ΔT Creep Test as a Parallelized Test Method
Examination of deformation rate effects using profilometry-based indentation plastometry
Exploring unusual Lüders deformation in UFG high-Mn austenitic steel
Finite element modeling of impacts for the measurement of material properties
High Temperature Profilometry-based Indentation Plastometry (HT-PIP) – Influence of Creep on Experimental Outcomes
Hydrogen assisted vacancy production and its effects on creep in structural steels
In-Situ Characterization Investigating Damage Propagation of SiC Composite Cladding
In-Situ Imaging of Spall Fracture
In-situ scanning electron microscopy testing of metallic materials: New methods & insights
In-Situ TEM Study on Toughening Mechanisms in Metal-Graphene Nanolayered Composites
In situ digital imaging correlation analysis of ultrasonic effects on dynamic and static strain aging
In Situ MicroCT Radiograph Corrections for Sub-Micron Scale Digital Volume Correlation
In Situ Nanomechanical Testing at Cryogenic Temperatures
Influence of Lattice Metamaterial Topology on Mechanical Response From Quasistatic to Shock Compaction Regimes
Influence of mechanical, thermal, and corrosive impacts on the performance of light metal structures and biomaterials
Influence of Non-Uniaxial Bending on Twinning and Phase Transformation in Molybdenum Nanowires
Influence of Unimodal and Bimodal γ' Precipitate Size Distributions on the Deformation Mechanisms in ATI 718Plus
Interfacial Plasticity of Nano-twinned Cu after Proton Irradiation
Investigation of Dislocation-Grain Boundary Interactions through In-Situ Direct Tensile Testing with High-Resolution Electron Backscatter Diffraction
Investigation of Size Effect in the Elastic Regime Through Micro-Scale Cantilever Bending Experiments
Kindling of burning particles to metallic substrates in high-pressure oxygen
Laboratory-scale simulation and combined modelling of hot multi-directional open-die forging and cogging
Macroscopic strain path dependence on the orientation and the distribution of microscopic strain localization in dual-phase steels
Mapping Strain, Stress and Orientation in Metals in 3D
Microstructural impact on brittle fracture path investigated via high-energy synchrotron techniques
Microstructure and Mechanical Property Correlation of Multi-Component Materials using the PI 89 Auto SEM PicoIndenter
Modeling Laser-Induced Microparticle Acceleration using A Mesoscale-Continuum Approach
Neutron Residual Stress Characterization: new steps towards harmonization and standardization
Nitrogen Hardening and its Resistance to Aging in a Martensitic Nitrided Steel Investigated by High Speed Nanoindentation
Per-grain behaviour in a duplex-steel during stress induced phase transformations
Phase Field Microelasticity Theory and Modeling of Dislocation Dynamics in an Elastically and Structurally Inhomogeneous Solid
Phase field modeling of slip transfer in thick biphase interfaces in HCP/BCC nanolaminates
Programming the Crack Propagation and Toughness in Mechanical Metamaterials
Quantifying the response of metals at elevated temperatures and strain rates above 106 s-1
Real-time sub-microscopic observation and atomic simulation of deformation-induced martensitic transformation at grain boundaries
Severe Plastic Deformation, Equal-Channel Angular Pressing, Commercially Pure Aluminium, Tribological Properties, Wear Loss, Coefficient of Friction, Design of Experiments
Small-scale mechanical testing of material properties enabled by site-specific femtosecond laser machining
Spatial and Temporal Deformation Behaviour of Hybrid Wrought – Additively Manufactured Inconel 718
Stochastic direct modeling of mechanical and thermal properties of polycrystals
Strain Rate Dependence of Activation Volume in Au Ultrafine Grained Thin Films Investigated by In Situ TEM
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Strength and deformability in nanolaminates containing thick 3D Interfaces
Superelastic behavior in shape memory alloys studied by in-situ SEM and TEM nano-compression and nano-tensile tests.
Tensile deformation behavior of polycrystalline pure cobalt with HCP / FCC dual phase studied by in-situ X-ray diffraction
The Development of the Δσ Parallelized Creep Test
The effect of β phase stability on the cyclic transformation behaviour metastable Ti alloys
The influence of concurrent structural mechanics and fluid flow in microstructure solidification modelling
The Role of Precipitates on Cyclic Stability of NiTi and NiTiCu Shape Memory Alloy Thin Films
Thermo-Mechanical Performance of Composite Metal Foams
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