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Meeting MS&T24: Materials Science & Technology
Symposium Manufacturing and Processing of Advanced Ceramic Materials
Presentation Title Fabrication of Continuous Polycrystalline Silicon Nitride (Si3N4) Fibers via Powder Processing Route
Author(s) Hyunjun Kim, Michael Cinibulk, Lisa Rueschhoff, Randall Hay, William Costakis , Connor Wyckoff, Seamus McGarvey, Randall Corns, Kathryn Rutherford, Brian Sirn
On-Site Speaker (Planned) Hyunjun Kim
Abstract Scope Ceramic matrix composites (CMC) currently rely on Al2O3 and Al2O3/mullite oxide fibers in the NextelTM family produced by 3M, or SiC fibers produced by Japanese companies. These fibers are not optimal for CMCs for RF applications – the dielectric constant for SiC is too high and use temperatures for Nextel fibers are too low. Si3N4 has a dielectric constant of 7.5, and high temperature stability comparable to SiC. Introduction of porosity into the Si3N4 reduces its dielectric constant as low as 2.3. To compensate low strength of porous Si3N4, its fiber has been sought as a fiber reinforcement but Si3N4 fiber is not available commercially. AFRL/RXNC has developed processes for making polycrystalline YAG fibers and can easily adapt the processes for YAG fiber to prepare Si3N4 fibers. Detailed fabrication process of continuous polycrystalline Si3N4 fiber will be presented and its properties will be discussed.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Critique of Additive Manufacturing of Ceramics
A Strategic Roadmap for Energy-Relevant Harsh Environment Material Research and Development Investments
Accelerating Experimental Determination of Multicomponent Transition Metal Carbide Phase Diagrams Using Uncertainty Quantification
Advanced Fuels by Field Assisted Sintering Technology – Fuel Properties and Accident Tolerance
Basic Materials Research Opportunities from the Army Research Laboratory
Bayesian Methods in Computational Thermodynamics with Applications in High-Temperature Ceramics
Controlling Abnormal Grain Growth in Ceramics
Correlation of Pore Size Distribution with Particle Size and Processing
D-11: Near-Room-Temperature Fabrication for Oxides by Acid-Base Chemical Densification and High-Throughput Powder Experiment Using Various Automated Tools
D-12: The Effect of Particle Size on Sintering Characteristics of Non-Pyroplastic Deformation Porcelain
Design and Manufacturing High-Entropy Li-Garnet Ceramic Electrolyte for Batteries
Design and Manufacturing of Sustainable Materials
Effect of Rapid Sintering Techniques on Defect Formation and Electrochemical Characteristics of Solid-Oxide Electrolysis Cell (SOEC) Materials
Effect of Suspension Solid Concentration on Physical Properties of Diverse Different Geometry UHTCs
Electric Field Assisted Sintering of Advanced Materials at Industrially Relevant Length Scales
Electrification of Ceramics Manufacturing
Enhanced Thermal Conductivity Using Segregated Thermal Pathway in Magnesia Composites
Fabrication and Characterization of Cs2HfCl6 Ceramics
Fabrication of Continuous Polycrystalline Silicon Nitride (Si3N4) Fibers via Powder Processing Route
Flash Joining of Metal-Ceramic Multi-Layered Sandwich Structure
From Spark Plasma Sintering to Ultra-Fast Consolidation of Carbides
From Understanding Flash Sintering Mechanisms to Realizing Ultrafast Sintering without Electric Fields and Controlling Microstructures with Electric Fields
Grain Size Refinement of Additive Manufactured Ce-TZP Ceramics by Coupled Two-Step Pre-Sintering and HIP
Inter-Lanthanide Ternary Oxide ABO3 Synthesis by Polymeric Steric Entrapment
Lithium Storage Performance of Anti-Site Defects Influenced Nanostructured LiFePO4 for High-Power Applications
Low Energy Sintering Processing Routes for Ceramic Materials
Measurement of Glaze Thermal Expansion via Crazing
Microstructure Classification and the Microstructure State Space
Microstructure Development of Novel Composite Heating Elements for Steel Decarbonization
Mullite Formation in Porcelain – A Problem with Rietveld Analysis
Novel Cermet Waste Forms for Nuclear Applications
Pitch-Perfect Nanoceramics: Swinging for the Fences in Processing and Manufacturing for Energy and Environmental Nexus
Probabilistic Physics-Integrated Neural Differentiable Modeling for Isothermal Chemical Vapor Infiltration Process
Rheological Factors and Compact Microstructures of Pressure Cast Technical Ceramics
Rheology of Colloids in Non-Aqueous Suspensions and Determination of the Stability Mechanism
Sequential Design of Experiments for Opacified Fibrous Insulation in Hypersonic Applications
Sintering Behavior of Non-Shrinkage and Low Pyroplastic Deformation Porous Ceramics
Spark Plasma Sintering (SPS) of Polymer Derived Silicon Oxycarbide (SiOC)
Ultra-Fast CO2 Laser Sintering of Iron-Alumina Metal-Ceramic Materials
Ultra-Fast Laser Sintering of Ceramics and Machine-Learning-Based Prediction on Processing-Microstructure-Property Relationships
Uncertainty Analysis in CALPHAD-Informed ICME Frameworks
Understanding Influence of Porosity and Impurities on Thermal Conductivity of ZrB2-Based Ultra-High Temperature Ceramics Through Thermodynamic Modeling

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