Abstract Scope |
This study optimised synthesis and ablation efficiency of silicon carbide nanoparticles using pulsed laser ablation in liquid for electronic and biomedical applications. Various process parameters, including laser fluence, scanning speed, and ablation time, were systematically varied to assess their impact on ablation efficiency and NP properties. Statistical analysis identified optimal conditions: a 15 min ablation time, 0.5 m/s scanning speed, and 7.5 J/cm² laser fluence with the maximum mass productivity of 1.196 mg.h−1W−1. Characterisation techniques, including UV-Vis, Dynamic Light Scattering (DLS), FESEM with EDX, FTSEM, and XRD, confirmed that higher laser fluence, scanning speed, and ablation time increased colloid concentrations without altering NP shape or size. XRD analysis verified the phase composition as 3C SiC, with DLS showing smaller NP sizes than image analysis. The results also suggested that increasing the NP size decreased the optical band gap. A direct correlation was found between ablated mass and colloid concentration. |