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Meeting MS&T24: Materials Science & Technology
Symposium Solid-State Transformations Under Complex Thermal Conditions
Presentation Title In-Situ Heating in Transmission Electron Microscopy to Characterize Nuclear Fuel
Author(s) Fidelma Giulia Di Lemma, Daniele Salvato, Kourtney Wright, Laura Hawkins, Kaustubh Bawane, Tiankai Yao, Luca Capriotti, Sriram Vijayan
On-Site Speaker (Planned) Fidelma Giulia Di Lemma
Abstract Scope During nuclear reactor operations the fuel experiences a harsh environment, due to intense radiation, material interaction and complex thermal conditions. Traditional studies of fuel performance have focused on post-irradiation examinations, which characterize the fuel only after reactor shutdown. Such postmortem characterization, usually performed at room temperature, limits our ability to understand the dynamics of phase transition and fuel microstructural evolution. Improvements in understanding can provide important input to material performance and can be utilized to improve fuel fabrication processes. Our recent studies have utilized in-situ transmission electron microscopy to characterize fuel in prototypical thermal reactor conditions. In-situ heating devices have been used to test fuel under steady state and under prototypical reactor thermal gradients. This talk will present new results focusing on microstructural changes in fuel such as grain structure evolution, phase reversion and elemental diffusion and interaction.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Additive Manufacturing of Beta Titanium Alloys: Influence of Thermo-Kinetics on Solid State Precipitation (Invited)
Design and Function of a Nanocalorimetry Sensor for In-Situ TEM Imaging
Effect of Partial Transformation Cycling on Transformation Behaviour of a Binary Nickel-Based Alloy
In-Situ Heating in Transmission Electron Microscopy to Characterize Nuclear Fuel
Multi-Stimuli Integration in Alloy Design: A Shear-Assisted Processing Approach for High-Performance Nano-Composite Materials
Predicting Emergence of Nanoscale Order in Surfaces Oxides Through Preferential Interactivity Parameter
Thermal Fatigue of Sn-Based Solders in Heterogenous Integration in Packaging (HIP) by Time-Resolved X-Ray Microscopy
Towards Predictive Microstructural Design of Additively Manufactured Metals
Using the SEAQT Framework to Predict the Kinetics of Irradiating an FeCr Alloy

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