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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Advances in Magnetism and Magnetic Materials
Presentation Title Correlative Microscopic Analysis of Grain Boundary Engineered Nd-Fe-B Permanent Magnets
Author(s) Pradeep Konda Gokuldoss
On-Site Speaker (Planned) Pradeep Konda Gokuldoss
Abstract Scope Nd-Fe-B magnet has been one of the most sought-after permanent magnetic materials for major energy applications due to its exceptional combination of magnetic properties. In specific, the coercivity of the Nd-Fe-B magnet can be increased by optimizing the microstructure, including reducing the grain size and by tuning the grain boundary chemistry. Accordingly, alloying of Nb to the Nd-Fe-B magnets restricts the grain growth by the formation of nano-scale Nb clusters. Further, low melting eutectics can be utilized, to decorate the grain boundaries (GB) of the Nd-Fe-B magnets which enables in increasing the coercivity of the magnet. To understand the process of GB diffusion on the Nd-Fe-B magnets, a custom designed correlative microscopy platform was utilized which facilitates combined transmission Kikuchi diffraction and Atom Probe Tomography. This correlative methodology applied to GB engineered commercial magnets, provided deeper insights into the role of microstructures on the final magnetic properties of the magnets.
Proceedings Inclusion? Planned:
Keywords Magnetic Materials, Phase Transformations, Characterization

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Additive Manufacturing of Thin-Walled Magnetocaloric Regenerator Structures for Heat Pump Applications
B-10: Evolution and Effect of Nd6Fe13Si-type Grain Boundary Phase on the Coercivity of Nd-Fe-B Sintered Magnet
B-11: Investigation of Ultra-High-Performance Soft Magnetic Materials with Controlled Nanocrystal Growth Through Nucleation-Dominant Composition Design
B-12: Magnetocaloric Effect for Gd(Mn,Fe,Co)Si Alloys
B-13: Medium Entropy Fe-Co-Ni-B-Al Alloys Obtained by Spark Plasma Sintering
B-14: Synthesis and Magnetic Evaluation of Carbonaceous Spinel Ferrite Nanocomposites
B-44: Thermodynamic Investigation of Rare-Earth Reduced Magnet Systems
B-9: A Study on the Improvement of Coercivity of Nd-Fe-B Permanent Magnets by GBDP of Ternary Alloy
Characterization of Crystallographic and Magnetic Domain Structures in Magnetic Alloys Using Complementary TEM Techniques
Combinatorial Synthesis and Characterization of New, Stable Mn-, W-, Hf-, and Nb-Based Ternary Nitrides
Correlative Microscopic Analysis of Grain Boundary Engineered Nd-Fe-B Permanent Magnets
Developing Domestic Supply Chains for Permanent Magnet Manufacturing
Development and Crystallography of fcc-bcc and bcc-fcc Precipitation in Soft Magnetic HEAs
Discovering New Functional Magnetic Materials Through High-Throughput Methods
Effect of Dy Substitution at Nd Sites in Melt-Spun Nd-Fe-B Permanent Magnet Ribbons: A Magnetic System for Electric Vehicles
Effects of Interstitial Elements on the Ordered Structure of Fe-Ni Alloys
Enhanced Mass Sensitivity of Self-Biased Magnetoelastic Sensors by Annealing-Induced Nanocrystallization
Experiments in Pulsed Magnetic Fields: A Powerful Tool to Study Multicaloric Materials
Fabrication of Alnico Permanent Magnets with Optimized Microstructures via Magnetic-Field-Assisted Direct Energy Deposition
First-Order Ferromagnetic Transition in MnFe(P,Si) Single Crystals
Grain Size Optimization for Sm2Fe17N3
Harnessing Interfacial Interactions in Perovskite Oxide Heterostructures
High-Throughput Design and Discovery of Novel Magnetic Nitrides
Influence of Applied Magnetic Field on the Nature of First-Order Phase Transformations in R2In Cryogenic Magnetocaloric Materials
Influence of Spinodal Decomposition on the Magnetic Properties of Additively Manufactured Alnico
Influence of Synthetic and Washing Protocols on Phase Purity and Magnetic Properties of Nd2Fe14B Powders Prepared by Calciothermic Reduction
Influencing Phase Development in Ferromagnetic Materials: Theory versus Practice
Internal Defect Detection and Characterization of Sm-Co Sintered Magnets by Ultrasonic Testing and Related Magnetic Properties
Investigation of Magnetron Sputtered Al0.25CrFeCoNi Thin Films for Enhanced Magnetic Properties
Iron Nitride Permanent Magnets
Linking Quantum Mechanical Features to Structural Phase-Transformation in Inorganic Solids
Magnetic and Mechanical Hardening of Nano-Lamellar Magnets Using a Thermo-Magnetic Field
Magnetic and Nano-Indentation Behavior in FeNi Invar Alloys
Magnetic High Entropy Oxide for Water Pollutant Degradation
Magnetic Iron Disilicide Nanostructures: Computational Studies
Magnetic Model Informed Design of Architected Permanent Magnets for Electric Machines
Magnetic Properties of Sm2Fe17N3 at Low Temperature
Magneto-Optics, Revisited
Magnetocaloric Properties of LaFe11.5Si1.5 Alloys with Cobalt and Nickel Substitutions
Microstructure-Property Relationship for Hot Deformed Fine-Grained NdFeB Magnet with High Magnetic Properties Through Two-Step Spark Plasma Sintering
New Fe-rich Ferromagnets Without Critical Elements
Powder Consolidation of Ce-Based Permanent Magnets
Processing and Magnetic Properties of Nd/PrFeB Ring Magnets Produced by Extrusion
Protecting Ultrafine Grained Dy-Free Nd-Fe-B Sintered Magnets with Varied Passivation Techniques
Rotating Magnetocaloric Effect in Polycrystals: Fundamentals and Applications
Smart Microactuators Based on Shape Memory Heusler Microwires
Soft Magnetic Materials for Motor Applications
Structural, Magnetic and Mechanical Characterization of Fe-Co-Ni-B-Ti Powder Medium-Entropy Alloys
Studies of Sintered Nb-Doped MM-(FeCo)-B-Based Magnets with the Addition of RE-Cu Grain Boundary Modification Alloys
Sustainable Magnets for Green Energy
Synthesis and Characterization Magnetic Membranes Based on PVA-SPION for Hyperthermia and Dielectric Applications

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