About this Abstract | 
  
   
    | Meeting | 
    2025 TMS Annual Meeting & Exhibition
       | 
  
   
    | Symposium 
       | 
    Advances in Magnetism and Magnetic Materials
       | 
  
   
    | Presentation Title | 
    Microstructure-Property Relationship for Hot Deformed Fine-Grained NdFeB Magnet with High Magnetic Properties Through Two-Step Spark Plasma Sintering | 
  
   
    | Author(s) | 
    Ziyi  Wu, Dong  Zhao, Baozhi  Cui, Lian  Jie | 
  
   
    | On-Site Speaker (Planned) | 
    Ziyi  Wu | 
  
   
    | Abstract Scope | 
    
Hot-deformed Nd2Fe14B-based magnets have attracted much research interest due to its potential high coercivity while eliminating heavy rare earth (HREE) elements. Conventional melt-spun HREE-free Nd-Fe-B ribbons with an isotropic nanograin (~50 nm) are used to manufacture hot-deformed anisotropic NdFeB magnets. It was found that controlling abnormal grain growth and achieving a high aspect ratio of fine-grains during hot deformation is critical to obtaining both high coercivity and (BH) max. In our study, we developed a novel two-step process using spark plasma sintering (SPS) to manufacture high-performance magnets. Nd-Fe-B ribbons were first highly densified by a novel cold sintering at 350 °C and 300 MPa to preserve the nanosized grains. The bulk was then quickly hot-deformed at 710 °C until fully densified, resulting in an anisotropic fine plate-like grain microstructure. The magnet obtained an intrinsic coercivity Hci of 11.2 kOe, remanence Br of 14.2 kGs, and a (BH) maxof 47 MGOe. | 
  
   
    | Proceedings Inclusion? | 
    Planned:  | 
  
 
    | Keywords | 
    Magnetic Materials, Powder Materials, Process Technology |