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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Refractory Metals 2025
Presentation Title High-throughput design, synthesis, and characterization of refractory multi-principal element alloys (MPEAs)
Author(s) Cafer Melik Ensar Acemi, Eli Norris, Brent Vela, Raymundo Arroyave, Ibrahim Karaman
On-Site Speaker (Planned) Cafer Melik Ensar Acemi
Abstract Scope Refractory alloys are promising for high-temperature applications because of their high strength at elevated temperatures, high thermal conductivity, low thermal expansion coefficient, and operability under oxidizing conditions. One hundred eighty-three refractory multi-principal element alloys (MPEAs) are designed under two sets of constraints to have single BCC phase at elevated temperatures, target yield strength (>200 MPa at 1300°C or >50 MPa at 2000°C), and narrow solidification range for additive manufacturability. Designed compositions are synthesized with high-throughput vacuum arc melting and characterized via electron microscopy (SEM/EDX), XRD, Vickers microhardness, nanoindentation, compression, and tension. In the as-cast state, the majority of samples had BCC phase with dendrites. Homogenization heat treatments are performed at 1800°C and 2000°C to eliminate dendritic structure after diffusion calculations based on the compositional differences measured in the dendrites. Compression/tension experiments are then performed at high temperatures to compare with the predicted high-temperature properties.
Proceedings Inclusion? Planned:
Keywords Characterization, High-Entropy Alloys, High-Temperature Materials

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Application of High Temperature Profilometry-based Indentation Plastometry (HT-PIP) to Refractory Metals
Assessment of State of the Art in Refractory Niobium Alloys
Characterizing recrystallization in Type 2 and Type 5 Nb
Creep resistant refractory multiple-principal-element alloy
Designing Refractory Alloy Bond Coats that Develop Thermally-Grown Complex Oxides: An Investigation of the Cr-Ta System
Effect of Geometric Features on Liquid Metal Dealloying of Additively Manufactured Niobium-Titanium
Effect of Microstructure on Machining Pure Tungsten
Evaluating Microstructure and Strength Properties of Tungsten based Refractory Multi-Principal Element Alloy fabricated by Laser Based Directed Energy Deposition
Exploring the Mo-Re Alloy System by Nanoindentation
Fabrication of Mo-Si-B alloy through spark plasma sintering using Mo powder containing La2O3 nanoparticles uniformly dispersed via ultrasonic spray pyrolysis
Fatigue crack propagation in semi-brittle materials: A case study on tungsten
Flow Stress and Microstructural Evolution of TZM and Mo-La Alloys at Temperatures from 1400 to 1700 °C
Get Low: Achieving Ultra-Fine Grain Sizes in Niobium with High-Pressure Torsion
Heat Treatment Optimization of Laser Powder Bed Fusion Additive Manufacture C103
High-temperature deformation in Nb-based alloy C103 (Nb-10Hf-1Ti)
High-Temperature Oxidation Behavior of Novel Refractory Complex Concentrated Alloys
High-throughput design, synthesis, and characterization of refractory multi-principal element alloys (MPEAs)
Investigating the Microstructure and High-temperature Mechanical Properties of Additively Manufactured W-Re Alloys
Low temperature oxidation behavior of pure niobium and C103 niobium alloy
Mechanical Behavior of Neutron Irradiated Ta-W Alloy
Microstructural Evolution of Nb-Alloys Produced via High-Pressure Torsion
Microstructure and mechanical properties of a Mo-Si-B-Ti alloy manufactured by laser powder bed fusion
New microscopic insights on the high temperature deformation mechanisms in refractory metals and alloys
Observations on surface deformation of tungsten materials in laser focus in air
Oxidation of refractory metals in molecular and dissociated oxygen
Preparation of Spherical Tungsten Alloy Powder with Particle Atomic Layer Deposition
Refractory alloy-based bimetallic structure fabricated by wire arc additive manufacturing
Refractory Alloy Microstructure Development with Processing Variations
Refractory Metals, A Nanocrystalline Approach
Systematic exploration of refractory high entropy alloys using high-throughput techniques and machine learning
Temperature Dependent Deformation in Single Crystalline MoNbTi
The development of new thermodynamic databases for niobium and molybdenum alloys
The High Temperature Performance of Mechanically Processed Equiatomic NbTaV Refractory Alloy
The oxidation behavior and mechanical properties of model Nb-Si-based alloys at elevated temperatures
Understanding the microstructural evolution and mechanical property in as-cast and annealed Refractory High Entropy Alloys

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