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Meeting 2023 TMS Annual Meeting & Exhibition
Symposium Methods, Techniques, and Materials Discovery of Irradiation Effect Using In-situ Microscopy
Presentation Title Advanced In Situ Mechanical Testing Approaches to Evaluate the Degradation of Nuclear System Components
Author(s) Maxim Gussev, David McClintock, Kevin Field, Ercan Cakmac, Travis Dixon
On-Site Speaker (Planned) Maxim Gussev
Abstract Scope In the recent two decades, common mechanical testing techniques showed significant progress, being coupled with advanced tools like EBSD. The present work combines own authors’ results and a limited literature review to discuss the advantages, challenges, and limitations of several advanced experimental approaches for testing irradiated specimens. In-house manufacturing of irradiated specimens is described in detail. Among the discussed experimental techniques of special focus are: (1) SEM/EBSD, allowing for investigating strain-induced phenomena, like lattice rotation, twinning, phase instability, and cracking; (2) Digital image correlation (DIC) with focus on in-SEM applications (µDIC). Examples are given, including a technique based on imaging radiation-induced voids via BSE contrast; (3) High-resolution EBSD (HR-EBSD). The approach relies on an in-depth analysis of diffraction patterns to retrieve in-grain stresses and local dislocation densities; (4) In-situ X-ray tomography, allowing for detecting and tracking pores, cracks, and discontinuities in the specimen volume.
Proceedings Inclusion? Planned:
Keywords Nuclear Materials, Mechanical Properties, Other

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Advanced In Situ Mechanical Testing Approaches to Evaluate the Degradation of Nuclear System Components
Deep Learning Defect Detection in Electron Microscopy of Radiation Damage in Metals
Discovering the Mechanisms of Helium Channel Evolution Via In-situ Annealing and Observation in TEM
Effect of Stacking Fault Energy on Microstructural Evolution of Compositionally Complex Alloys under In situ Dual-beam Heavy-ion Irradiation
Evolution of Vacancy/Interstitial Dislocation Loops in Pure Zr and Ti at Elevated Temperatures Observed by In-situ TEM Annealing
Helium Effects on Defect Evolution of In-situ Irradiated Additive-manufactured Grade 91 Steel
High Throughput Assessment of Advanced Nuclear Materials via In-situ TEM
In-situ 3D High-energy X-ray Diffraction Study on Deformation Behavior of Neutron-irradiated Fe-9%Cr
Industrial Nuclear Materials Applications for In-situ Microscopy
Is a TEM Foil “Bulk Enough” to Study the Parabolic Air-ingress Oxidation of W PFM in In-situ Environmental TEM?
Laboratory-based 3D X-ray Imaging of Neutron-irradiated TRISO Fuel
Observations of ‘Far from Equilibrium’ Phenomena under in Reactor Thermal Conditions Using In Situ TEM
Particle-induced X-ray Emission Spectroscopy (PIXE) for In Situ Monitoring of Corrosion Under Proton Irradiation in the Irradiation-corrosion Experiment (ICE)
Perspectives on Quasi-in-situ Characterization of Nuclear Materials Using Synchrotron X-rays
Precipitate and Cavity Evolution in Alloy 718 Under High Temperature In-situ Ion Irradiation using Machine Learning
Quantifying the Recovery of Irradiated and Cold-worked Zr-2.5Nb Using X-ray and Neutron Diffraction Line Profile Analysis
Radiation Tolerance of Amorphous Alumina Cladding Coatings for Heavy Liquid Metal Cooled Fast Reactors: Temperature and Dose Effect.
Rare-earth Titanates Ln2TiO5 Crystal Chemistry and Radiation Response. A Review.
Revealing 3D Microstructures in Nuclear Materials with High-energy X-rays
Revealing Heat-treatment Induced Stoichiometric Variations in Neutron-irradiated Yttrium Hydrides Using In Situ Synchrotron Radiation Diffraction
Simultaneous Proton Irradiation Changes Molten Fluoride Salt Corrosion Rates and Mechanisms
Transient Grating Spectroscopy of Defect Annealing Kinetics and Microstructural Evolution in Self-ion Implanted Tungsten with In-situ Annealing
Uncovering Transient Grain Boundary Absorption States Using Deep Learning Object Detection
Understanding the Amorphization Limit in Irradiated Ceramics via Repeated In situ Recrystallization Experiments
Utilizing High-energy X-rays for Microstructural Characterization of Metallic Hydrides

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