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Meeting MS&T24: Materials Science & Technology
Symposium Additive Manufacturing of Ceramic-based Materials: Process Development, Materials, Process Optimization and Applications
Presentation Title Irradiative Ceramization of Chemically Bound Phosphate Ceramics (CBPCs) to Enable Direct Additive Manufacturing of Ceramic Composites
Author(s) Mark D. Losego
On-Site Speaker (Planned) Mark D. Losego
Abstract Scope This talk will introduce a rapid, pressureless process to chemically bind ceramic parts via a combination of inorganic phosphate chemistries and electromagnetic irradiation. The ceramic components are synthesized from slurries of ceramic powders and Al(H2PO4)3 binders. In initial studies, short-waved IR irradiation drives phosphate condensation reactions, however under these low irradiation powers (~0.2 W/cm2), condensation and ceramization requires minutes to tens of minutes to complete. Using a high-power flash lamp annealing (FLA) system (~10 kW/cm2) enables rapid ceramization in under 1 min and denser overall microstructures. Interestingly, though, the total irradiation energy required to drive complete ceramization is similar for both processes. The talk will also discuss the importance of light absorbers and the development of printed, high-temperature thermochromic ceramic sensors using this new additive manufacturing approach.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Dense Complex Shape Ceramic Components Fabricated By Digital Light Printing (DLP) and Liquid Silicon Infiltration (LSI)
Densification and Microstructure Evolution of Alumina Structures via Direct Ink Writing
Density Improvement of Binder Jet Printed MnZn Ferrite Cores via Pre-and Post- Sintering Improvement Strategies
Direct Ink Writing of SiOC Structure from Preceramic Polymer Containing Inactive Fillers
Dispersion of PMN-PZT for Direct Ink Writing
Fused Filament Fabrication of Ceramic Matrix Composite Preforms Via Thermo-Oxidative Stabilization of Polyetheretherketone
Interface Stability of Iron-Carbide Materials Fabricated via Laser-Direct Energy Deposition
Irradiative Ceramization of Chemically Bound Phosphate Ceramics (CBPCs) to Enable Direct Additive Manufacturing of Ceramic Composites
Laser-Directed Energy Deposition Additive Manufacturing of Lunar Highlands Simulant (LHS-1) Lunar Regolith Simulant for In Situ Resource Utilization
Multi Ceramic Additive Manufacturing Based on Novel Digital Light Processing Technology
Optimizing SiC Slurries for Robocasting High-Performance SiC.
Rapid Volumetric Microwave Curing of Silicon Nitride Ceramic Binder Mixtures
Stabilization of Alumina Dispersed Slurry by Controlling pH
Towards Direct Additive Manufacturing of Bulk Ceramics Using Selective Laser Flash Sintering
Use of 2D Ti3C2 MXene as an Additive in SiC and Their High-Temperature Phase Behavior
Using Laser Ultrasonics to Correlate Young’s Modulus to Particle Neck Size in Early-Stage Sintering

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