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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Spectroscopic Methods and Analysis for Nuclear Energy Related Materials
Presentation Title Correlative multi-modal analysis of nuclear graphite deformation mechanisms
Author(s) Thomas Zillhardt
On-Site Speaker (Planned) Thomas Zillhardt
Abstract Scope Graphite plays a pivotal role in the safe and efficient operation of nuclear reactors. It is essential for maintaining structural integrity, effective thermal management, and providing neutron moderation. The variety of graphite grades and the challenging reactor operating conditions require leveraging novel correlative X-ray and neutron methods in situ to investigate the microstructural and mechanical properties of nuclear graphite, aiming to enhance its performance and longevity under reactor conditions. In-situ high-speed tomography, combined tomography and diffraction stress measurements, in-situ neutron Bragg imaging and scattering have been developed and applied at international research facilities including Diamond, STFC-ISIS, ESRF, ILL and Soleil to investigate crystal reorientation, crack initiation and coalescence, brittle fracture, and notch sensitivity. By integrating data from X-ray and neutron methods, researchers can develop a more holistic understanding of the material's behaviour, critical for improving predictive models and guiding the development of advanced graphite grades with enhanced performance.
Proceedings Inclusion? Planned:
Keywords Characterization, Nuclear Materials, Other

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

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Atomic-scale structural analysis of metastable zirconia
Complementarity of Neutrons and Positrons in Assessing Material Damage for Nuclear Applications
Correlative Investigation of Hydride Phase Formation and Transformation in Zircaloy-4 Using In Operando XRD and Feature Relocation EBSD-SEM
Correlative multi-modal analysis of nuclear graphite deformation mechanisms
Examination of U19Pu10Zr fluff structure by X-ray tomography and time-of-flight secondary ion mass spectrometry
In-situ Synchrotron Diffraction Investigations of a Scalable, Non-equilibrium Processing Route of ODS Steels for Nuclear Power
In situ helium implantation and Rutherford backscattering analysis of helium retention in amorphous SiOC
Investigating nuclear materials via laser based and positron annihilation spectroscopy techniques to understand their performance
Investigation of Local Defects in Ln-doped UO2: Impact of Fabrication Condition and Lanthanide type
Nano-scale Orientation Mapping Using Electron Backscatter Diffraction
Nanostructural Characterization of Electron Beam Welded Reactor Pressure Vessel Steel via XANES and Nano-CT
Nuclear Materials Research at the Synchrotron
Observing radiation enhanced diffusion in model Fe-Cr alloys and their oxides using atom probe tomography
Quantification of total irradiation damage in nuclear graphite using Raman spectroscopy
Revealing the Crystal Chemistry and Dissolution Kinetics of Doped Uranium Dioxide Nuclear Fuel
Studying the use of x-ray line profile analysis in irradiated materials via atomistic simulations
Synchrotron Characterization of Uranium Boride Alloyed with Chromium Oxidation Behavior
The Surprising Beneficial Effect of Low-Dose Proton Radiation on Suppressing the Corrosion Reactivity of Thermally Oxidized Iron
The use of spatially resolved EELS spectroscopy to elucidate irradiation induced phase transformation in Fe2O3 and Cr2O3 irradiated with ions and its impact on irradiation induced-loop formation
ToF-SIMS Characterization of Irradiated U-Zr FCCI Region Using Spectra Clustering
Vapor analysis by combination spectroscopy in a novel optical cell
X-Ray Diffraction-Computed Tomography (XRD-CT) Facility at NSLS-II for Studying Materials for Nuclear Applications

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