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Meeting Materials Science & Technology 2020
Symposium Sintering and Related Powder Processing Science and Technologies
Presentation Title Grain Growth Measurements of Anti-thermal Strontium Titanate with Non-destructive High Energy X-ray Diffraction Microscopy (HEDM)
Author(s) Amanda Krause, He Liu, Christopher J Marvel, Bryan Conry, Michael Hoffmann, Robert Suter, Carl E Krill, Martin P Harmer
On-Site Speaker (Planned) Amanda Krause
Abstract Scope Strontium titanate (SrTiO3) exhibits anti-thermal grain growth between 1350°C and 1425°C, where the grain boundary mobility decreases as the temperature increases. The underlying mechanism for this rare grain growth behavior is unknown. Previous grain growth studies show a change in the grain boundary character distribution within this temperature range. However, conventional grain growth studies rely on statistical comparisons of grain size distributions to describe grain growth and cannot capture the migration of individual grain boundaries or those of a specific energy or character. Here, the non-destructive microstructural characterization method high-energy x-ray diffraction microscopy (HEDM) is employed to directly correlate the velocity and character of individual SrTiO3 grain boundaries to elucidate anti-thermal behavior. Initial observations and the grain boundary velocity measurements at 1350°C (thermal regime) and 1400°C (anti-thermal regime) will be discussed.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Coarsening of Several Ceramic Particle Systems
Electron Microscopy Observation of Electric Field Assisted Sintering of Stainless Steel Nanoparticles
Flash Sintering Solid State Ceramic Electrolytes Using a Novel Multi- electrode Approach
Grain Growth Measurements of Anti-thermal Strontium Titanate with Non-destructive High Energy X-ray Diffraction Microscopy (HEDM)
Novel Low-temperature Copper Sintering Paste for Large-area Die Attachment at 200 ℃ in Nitrogen Atmosphere
On the Bending of High-aspect Ratio Freestanding Aerosol Jet Printed Micropillar Arrays during Thermal Sintering
Reduced Pressure Nanosintering during Environmentally Controlled – Pressure Assisted Sintering
Selective Sintering Technique: Modeling and Experimentation
The Effect of Cryogenic Milling and Parameters of Spark Plasma Sintering on Microstructure, Phase Composition and Mechanical Properties of Metastable Beta Titanium Alloy Ti-15Mo
The Effect of Texturing by Applied Magnetic Field on Grain Growth of Alumina

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