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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Characterization of Materials through High Resolution Coherent Imaging
Presentation Title AI-Driven Workflow for Autonomous High-Resolution Scanning X-Ray Microscopy
Author(s) Tao Zhou, Saugat Kandel, Mathew Cherukara, Charadatta Phatak, Martin Holt
On-Site Speaker (Planned) Tao Zhou
Abstract Scope We report the Fast Autonomous Scanning Toolkit (FAST) that combines a neural network, route optimization, and efficient hardware controls to enable a self-driving experiment that actively identifies and measures a sparse but representative data subset in lieu of the full dataset. FAST requires no prior information about the sample and is computationally efficient. We demonstrate FAST in a dark-field X-ray microscopy experiment on an exfoliated multilayer WSe2 thin film. Our studies show that a FAST scan of <25% is sufficient to accurately image all the spontaneously formed bubbles in the sample, with a decision making time of less than 1 second per 50 points. FAST is easy to adapt for any scanning microscope. Its broad adoption will empower general multi-level studies of materials evolution with respect to time, temperature, or other parameters.
Proceedings Inclusion? Planned:
Keywords Machine Learning, Characterization,

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

AI-Driven Workflow for Autonomous High-Resolution Scanning X-Ray Microscopy
Bragg Coherent Diffractive Imaging With Twisted X-Rays
Characterization of Crystalline Materials at the Atomic Scale with X-Ray Bragg Coherent Diffraction Imaging
Coherent x-Ray Diffraction Imaging Dedicated Beamlines at PLS-II and Korea-4GSR
Direct Reciprocal Space Detection of Microelectronic Defects Using Coherent X-Ray Diffraction and Unsupervised Machine Learning
Enhanced Mineral Characterization With 3D X-Ray CT and AI-Driven Imaging
Explanation of the High-Dielectric Constant of BaTiO3 Used in Multilayer Capacitors
High-Resolution X-Ray Imaging of Integrated Circuits
High Bandwidth Scanning X-Ray Microscopy
In-Situ/Operando Bragg Coherent X-Ray Diffraction Imaging for Catalysis Studies
ML-Guided Non-Destructive 3D Metrology of Functioning Devices With an X-Ray Laser
Nanoholotomography With Coded Apertures for Efficient Dynamic Imaging of Nanomaterials
Operando and Linear Dichroic Ptychographic Spectro-Tomography of Heterogenous Catalysts
Origin of Structural Degradation in Layered Oxide Cathode for Li-Ion Batteries
Physics-Informed Self-Supervised Learning of Structural Morphology Imaged by Scanning X-Ray Diffraction Microscopy
Probing Cryogenic Strain Evolution in SrTiO3 Using Multi-Reflection Bragg Coherent Diffraction Imaging
Rapid Reconstruction of the Full Strain Tensor via Coupled Phase Retrieval With Multipeak Bragg Coherent Diffraction Imaging
Real-Time Imaging of Subsurface Dislocation Dynamics
Simultaneous Reciprocal and Real Space X-Ray Imaging for Hierarchical Characterization of 3D Nano-Architected Metamaterials
Single-Exposure Elemental Differentiation and Texture-Sensitive Phase-Retrieval Imaging with a Neutron-Counting Microchannel-Plate Detector
Single-Shot X-Ray Imaging of Density in Laser Shocked Materials for Fusion Energy Studies
Synchrotron Ptychographic X-Ray Computed Tomography (PXCT) to Study Micro-Fabricated Fully Hybrid 3D Metal-Ceramic Metamaterials
Three-Dimensional Hard X-Ray Ptychographic Reflectometry Imaging on Extended Mesoscopic Surface Structures

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