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Meeting TMS Specialty Congress 2025
Symposium Joint Sessions of AIM, ICME, & 3DMS
Presentation Title Innovations in 3D EBSD for Advanced Materials Characterization
Author(s) Andrew Polonsky, Chad Hovey, James Lamb, Paul Chao, McLean Echlin, Hojun Lim, Kyle Johnson, Julia Deitz, Tresa Pollock
On-Site Speaker (Planned) Andrew Polonsky
Abstract Scope Recent advancements in automation have transformed materials characterization techniques over the past decade. The capability to perform serial-sectioning within an electron microscope using ion or laser beams has facilitated the acquisition of high-fidelity 3D electron backscatter diffraction (EBSD) data, resulting in increasingly large datasets. Here we explore the application of 3D EBSD to analyze microstructures obtained through serial-sectioning with the TriBeam system, revealing insights into these materials that traditional methods cannot provide. We will address analytical considerations for non-equilibrium microstructures, such as those produced by macroscopic plastic deformation or additive manufacturing. Additionally, we will outline workflows for automated management of multi-terabyte datasets and present novel collection and analysis tools designed to minimize the reliance on specialized knowledge, thus making this advanced technique more accessible to a broader audience. Furthermore, we will discuss how these datasets can be leveraged for advanced modeling techniques to enhance our fundamental understanding of materials processing.
Proceedings Inclusion? Definite: Post-meeting proceedings

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