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Meeting 2023 TMS Annual Meeting & Exhibition
Symposium Methods, Techniques, and Materials Discovery of Irradiation Effect Using In-situ Microscopy
Presentation Title In-situ 3D High-energy X-ray Diffraction Study on Deformation Behavior of Neutron-irradiated Fe-9%Cr
Author(s) Dominic Piedmont, Jun-Sang Park, Peter Kenesei, Jonathon Almer, Matthew Kasemer, Ezra Mengiste, James Stubbins, Meimei Li, Xuan Zhang
On-Site Speaker (Planned) Dominic Piedmont
Abstract Scope Given the extreme environments nuclear reactor core structural materials are exposed to, significant effort must be made to understand the microstructure-property correlation. However, there is a discontinuity of length scales under common investigation of materials. Mechanical testing provides insight to bulk behavior while electron microscopy gives nano- to micro-meter scale information. Presented is a direct link between the discontinuous length scales previously observed, via grain scale (meso-scale) characterization of deformation responses in irradiated materials. Using synchrotron x-rays, high energy x-ray diffraction microscopy (HEDM) nondestructively probes mm-size samples to obtain grain-resolved information in-situ and ex-situ. The resulting data allows for observations of grain rotation and residual strain evolutions as a function of deformation. Results were obtained for Fe-9%Cr samples: two irradiated to 0.1 dpa at temperatures of 300°C and 450°C, and one unirradiated sample for comparison. Experimental results are compared to computational results from Crystal Plasticity Finite Element Modeling (CPFEM) simulations.
Proceedings Inclusion? Planned:
Keywords Characterization, Mechanical Properties, Modeling and Simulation

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Advanced In Situ Mechanical Testing Approaches to Evaluate the Degradation of Nuclear System Components
Deep Learning Defect Detection in Electron Microscopy of Radiation Damage in Metals
Discovering the Mechanisms of Helium Channel Evolution Via In-situ Annealing and Observation in TEM
Effect of Stacking Fault Energy on Microstructural Evolution of Compositionally Complex Alloys under In situ Dual-beam Heavy-ion Irradiation
Evolution of Vacancy/Interstitial Dislocation Loops in Pure Zr and Ti at Elevated Temperatures Observed by In-situ TEM Annealing
Helium Effects on Defect Evolution of In-situ Irradiated Additive-manufactured Grade 91 Steel
High Throughput Assessment of Advanced Nuclear Materials via In-situ TEM
In-situ 3D High-energy X-ray Diffraction Study on Deformation Behavior of Neutron-irradiated Fe-9%Cr
Industrial Nuclear Materials Applications for In-situ Microscopy
Is a TEM Foil “Bulk Enough” to Study the Parabolic Air-ingress Oxidation of W PFM in In-situ Environmental TEM?
Laboratory-based 3D X-ray Imaging of Neutron-irradiated TRISO Fuel
Observations of ‘Far from Equilibrium’ Phenomena under in Reactor Thermal Conditions Using In Situ TEM
Particle-induced X-ray Emission Spectroscopy (PIXE) for In Situ Monitoring of Corrosion Under Proton Irradiation in the Irradiation-corrosion Experiment (ICE)
Perspectives on Quasi-in-situ Characterization of Nuclear Materials Using Synchrotron X-rays
Precipitate and Cavity Evolution in Alloy 718 Under High Temperature In-situ Ion Irradiation using Machine Learning
Quantifying the Recovery of Irradiated and Cold-worked Zr-2.5Nb Using X-ray and Neutron Diffraction Line Profile Analysis
Radiation Tolerance of Amorphous Alumina Cladding Coatings for Heavy Liquid Metal Cooled Fast Reactors: Temperature and Dose Effect.
Rare-earth Titanates Ln2TiO5 Crystal Chemistry and Radiation Response. A Review.
Revealing 3D Microstructures in Nuclear Materials with High-energy X-rays
Revealing Heat-treatment Induced Stoichiometric Variations in Neutron-irradiated Yttrium Hydrides Using In Situ Synchrotron Radiation Diffraction
Simultaneous Proton Irradiation Changes Molten Fluoride Salt Corrosion Rates and Mechanisms
Transient Grating Spectroscopy of Defect Annealing Kinetics and Microstructural Evolution in Self-ion Implanted Tungsten with In-situ Annealing
Uncovering Transient Grain Boundary Absorption States Using Deep Learning Object Detection
Understanding the Amorphization Limit in Irradiated Ceramics via Repeated In situ Recrystallization Experiments
Utilizing High-energy X-rays for Microstructural Characterization of Metallic Hydrides

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