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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Spectroscopic Methods and Analysis for Nuclear Energy Related Materials
Presentation Title Advanced synchrotron characterization techniques for fusion materials science
Author(s) David Sprouster, Takaaki Koyanagi, D Olds, M Ouyang, S Fayfar, E O'Quinn, M Lang, Y Yang, Y Lin, B Khaykovich, Y Katoh, Julie Tucker, J Trelewicz, Lance Snead
On-Site Speaker (Planned) David Sprouster
Abstract Scope Characterization methods capable of providing critical information across multiple structural length scales are essential in materials exposed to the extreme environments such as anticipated future fission and fusion power systems. Complementary techniques capable of uncovering the microstructural irradiation induced evolution are also important to verify and validate advanced computational models. In this presentation, we discuss our recent application of synchrotron-based x-ray scattering and absorption characterization methods in fusion and fission materials research. Specifically highlighted are opportunities in leveraging synchrotron-based techniques to address fundamental and applied materials science challenges at various length scales and in support of modeling efforts. Examples presented in this presentation include precipitate quantification in as-fabricated and as-irradiated fission-relevant steels and metallic alloys; microstructural quantification in neutron irradiated metal-hydrides for moderator applications; neutron irradiation induced structural degradation in ultra-high temperature ceramics; and quantification of the atomic structure of transmutation elements in tungsten-based plasma facing components.
Proceedings Inclusion? Planned:
Keywords Characterization, Nuclear Materials, Phase Transformations

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Advanced synchrotron characterization techniques for fusion materials science
Atomic-scale structural analysis of metastable zirconia
Complementarity of Neutrons and Positrons in Assessing Material Damage for Nuclear Applications
Correlative Investigation of Hydride Phase Formation and Transformation in Zircaloy-4 Using In Operando XRD and Feature Relocation EBSD-SEM
Correlative multi-modal analysis of nuclear graphite deformation mechanisms
Examination of U19Pu10Zr fluff structure by X-ray tomography and time-of-flight secondary ion mass spectrometry
In-situ Synchrotron Diffraction Investigations of a Scalable, Non-equilibrium Processing Route of ODS Steels for Nuclear Power
In situ helium implantation and Rutherford backscattering analysis of helium retention in amorphous SiOC
Investigating nuclear materials via laser based and positron annihilation spectroscopy techniques to understand their performance
Investigation of Local Defects in Ln-doped UO2: Impact of Fabrication Condition and Lanthanide type
Nano-scale Orientation Mapping Using Electron Backscatter Diffraction
Nanostructural Characterization of Electron Beam Welded Reactor Pressure Vessel Steel via XANES and Nano-CT
Nuclear Materials Research at the Synchrotron
Observing radiation enhanced diffusion in model Fe-Cr alloys and their oxides using atom probe tomography
Quantification of total irradiation damage in nuclear graphite using Raman spectroscopy
Revealing the Crystal Chemistry and Dissolution Kinetics of Doped Uranium Dioxide Nuclear Fuel
Studying the use of x-ray line profile analysis in irradiated materials via atomistic simulations
Synchrotron Characterization of Uranium Boride Alloyed with Chromium Oxidation Behavior
The Surprising Beneficial Effect of Low-Dose Proton Radiation on Suppressing the Corrosion Reactivity of Thermally Oxidized Iron
The use of spatially resolved EELS spectroscopy to elucidate irradiation induced phase transformation in Fe2O3 and Cr2O3 irradiated with ions and its impact on irradiation induced-loop formation
ToF-SIMS Characterization of Irradiated U-Zr FCCI Region Using Spectra Clustering
Vapor analysis by combination spectroscopy in a novel optical cell
X-Ray Diffraction-Computed Tomography (XRD-CT) Facility at NSLS-II for Studying Materials for Nuclear Applications

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