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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Spectroscopic Methods and Analysis for Nuclear Energy Related Materials
Presentation Title Complementarity of Neutrons and Positrons in Assessing Material Damage for Nuclear Applications
Author(s) Joe F. Kelleher
On-Site Speaker (Planned) Joe F. Kelleher
Abstract Scope Neutron scattering plays an established role in the analysis and development of structural materials, providing information over a range of length scales. Here, we report recent developments in characterisation techniques for types of material degradation relevant to the nuclear energy sector, in particular measuring material voids and defects from irradiation or the early stages of creep or fatigue. Positron annihilation methods offer a useful probe, but availability at central scientific facilities is currently limited. This is despite there being several demonstrated or conceivable implementations of the technique that would be relatively simple to deploy at existing neutron sources. Beyond this, we also consider ways in which the full diffraction spectrum acquired on a time-of-flight neutron instrument can provide a gauge of material damage or degradation, even where these spectra were recorded for the purpose of elastic strain measurements, thereby adding additional context for integrity assessments based on residual stress.
Proceedings Inclusion? Planned:

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Advanced synchrotron characterization techniques for fusion materials science
Atomic-scale structural analysis of metastable zirconia
Complementarity of Neutrons and Positrons in Assessing Material Damage for Nuclear Applications
Correlative Investigation of Hydride Phase Formation and Transformation in Zircaloy-4 Using In Operando XRD and Feature Relocation EBSD-SEM
Correlative multi-modal analysis of nuclear graphite deformation mechanisms
Examination of U19Pu10Zr fluff structure by X-ray tomography and time-of-flight secondary ion mass spectrometry
In-situ Synchrotron Diffraction Investigations of a Scalable, Non-equilibrium Processing Route of ODS Steels for Nuclear Power
In situ helium implantation and Rutherford backscattering analysis of helium retention in amorphous SiOC
Investigating nuclear materials via laser based and positron annihilation spectroscopy techniques to understand their performance
Investigation of Local Defects in Ln-doped UO2: Impact of Fabrication Condition and Lanthanide type
Nano-scale Orientation Mapping Using Electron Backscatter Diffraction
Nanostructural Characterization of Electron Beam Welded Reactor Pressure Vessel Steel via XANES and Nano-CT
Nuclear Materials Research at the Synchrotron
Observing radiation enhanced diffusion in model Fe-Cr alloys and their oxides using atom probe tomography
Quantification of total irradiation damage in nuclear graphite using Raman spectroscopy
Revealing the Crystal Chemistry and Dissolution Kinetics of Doped Uranium Dioxide Nuclear Fuel
Studying the use of x-ray line profile analysis in irradiated materials via atomistic simulations
Synchrotron Characterization of Uranium Boride Alloyed with Chromium Oxidation Behavior
The Surprising Beneficial Effect of Low-Dose Proton Radiation on Suppressing the Corrosion Reactivity of Thermally Oxidized Iron
The use of spatially resolved EELS spectroscopy to elucidate irradiation induced phase transformation in Fe2O3 and Cr2O3 irradiated with ions and its impact on irradiation induced-loop formation
ToF-SIMS Characterization of Irradiated U-Zr FCCI Region Using Spectra Clustering
Vapor analysis by combination spectroscopy in a novel optical cell
X-Ray Diffraction-Computed Tomography (XRD-CT) Facility at NSLS-II for Studying Materials for Nuclear Applications

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