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Meeting 2023 TMS Annual Meeting & Exhibition
Symposium Characterization of Materials through High Resolution Coherent Imaging
Presentation Title Exploring the Formation of Superlattice in Metal Nanocrystals using Bragg Coherent X-ray Diffraction Imaging
Author(s) Ericmoore E. Jossou, Ana Suzana, Longlong Wu, Jiecheng Diao, Tadesse Assefa, Steven Leake, Adam Gabriel, Anton Schneider, Kim Kisslinger, Lin Shao, Yongfeng Zhang, Lynne Ecker, Jian Gan, Ian Robinson, Simerjeet Gill
On-Site Speaker (Planned) Ericmoore E. Jossou
Abstract Scope Self-organization of defects in materials can create novel physical properties with potential applications in electronics and nuclear energy systems. In our work, we studied the physical mechanism of self-organization of krypton gas bubbles in nanocrystalline palladium under ion implantation. The formation of superlattices is affected by surface defects sinks which are predominant in nanocrystals compared to bulk metals. Using Bragg coherent X-ray diffraction imaging and transmission electron microscope, we determined the structure of the nanocrystal with the resolution sufficient to resolve each palladium nanoparticle. The reconstructed electron density of the nanocrystal reveals its intrinsic structural heterogeneity, including local deviations of lattice parameters, and the presence of internal defects. Variation in strain and lattice parameters and distribution of defects as a function of implantation conditions and fundamental mechanisms of noble gas ordering in nanocrystals compared to the bulk counterpart will be discussed.
Proceedings Inclusion? Planned:
Keywords Characterization, Other, Nuclear Materials

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

3D Nanoscale Crystalline Microscopy: The Interest of 3D Bragg Ptychography for Material Science
Advances in Phase Retrieval for In Situ Observation of Dislocation Dynamics in Gold Microcrystals
Catalytic Properties at the Nanoscale Probed by Coherent Diffraction Imaging
Characterisation of Material Defects via Plasmon-enhanced Phase Imaging
Coherent Surface Scattering Imaging with Nanometer Resolution for 3D Mesoscale Structures at Surfaces and Interfaces
Exploring the Formation of Superlattice in Metal Nanocrystals using Bragg Coherent X-ray Diffraction Imaging
Fluctuation Analysis of Coherent Electron Diffuse Scattering for Diffractive Imaging
High-speed Free-run Ptychography at the Australian Synchrotron
Imaging Intact Human Organs across the Scales using Hierarchical Phase-contrast Tomography
Imaging Laser Shockwave Dynamics in Defect-bearing Ablator Materials
In Situ and Operando 3D Imaging of Pt and Pd Electrocatalytic Nanocrystals
In Situ Bragg Coherent X-ray Diffraction Imaging Studies
Internal Strain Changes of Pt Nanoparticles in Response to the High Pressure in Diamond-anvil Cell
Method Developments for High-efficient X-ray Coherent Diffraction Imaging
MHz Microscopy at European XFEL
Nanoscale Imaging of Electrochemically-induced Strain Dynamics in a Locally Polarized Pt Grain
Near Atomic Resolution BCDI through Materials Modeling
Precise Registration Algorithm for High-resolution Imaging Applications
Rationalization of CO2 Adsorption on Ni nanocrystals using Bragg Coherent X-ray Imaging
Resolving the Morphology of a Polyphase Solidification Pattern via In-situ Nanotomography
Searching for Crystals, Twins, Peaks and Dislocations with BCDI
Solving Complex Structures with Electron Ptychography
Structural Evolution of Nanoparticles Under Realistic Conditions Observed with Bragg Coherent X-ray Imaging
The Application of Advanced Coherent Imaging Technique and Element Analysis on a Self-organized Loop Structure
Ultrafast Dark-field X-ray Microscopy – A New Tool for Multiscale Analysis
Using Automatic Differentiation to Solve the Phase Problem in X-ray Bragg Ptychography
"Similarity Mapping" Using Precession Electron Diffraction Data

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