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Meeting 2020 TMS Annual Meeting & Exhibition
Symposium Characterization of Minerals, Metals and Materials
Presentation Title Introducing 3D-LIBS, a Powerful Rapid Chemical Mapping Tool for Trace Elements in Complex Materials
Author(s) Carys P. Cook, Rajiv Soman, Karol Putyera
On-Site Speaker (Planned) Rajiv Soman
Abstract Scope Characterizing the distribution of trace elements in many advanced solid materials can be analytically challenging and time-consuming. 3D-LIBS (Laser Induced Breakdown Spectroscopy) is a powerful, rapid, quasi-simultaneous, and indirect micro-sampling technique that can identify and map any element (including light elements and gases) to 1 ppm, in most solid materials. Sample surfaces can be mapped over a variety of spatial scales, from 10’s of microns to centimeters, with depth resolutions of 100’s of nanometers to 10’s of microns. We investigate a range of materials for trace element distributions in film/coating/substrate interfaces or treated/exposed surfaces. Examples include, i) H, O, B, S and Ti in Ni superalloys, ii) O, H and alkali elements in high purity Al metal, iii) refractories in high refractive glasses, and iv) Li and metal distribution in Li battery electrodes.
Proceedings Inclusion? Planned:

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

3D Characterization of the Evolution of Crystal Mosaicity During Solidification of Single Crystal Ni-based Superalloys
A Bibliometric Analysis of the Strategy and Performance Measurement of the Polymer Matrix Nanomaterials Development Scenario Globally and the Participation of Brazil
A Differential Scanning Calorimetry Study of the Combustion Synthesis of Metal Hexaborides
A Fully Integrated In-Situ Solution for Materials Testing in Sem
A New Characterization Tool for 3D Orientation Microscopy at Mesostructure Length Scales
Accurate Determination of EBSD Pattern Centers with Applications in Resolving Pseudosymmetry
Activated Carbon Prepared from Bituminous Coal/poplar Blends by Direct KOH Activation
Advanced Approach in Investigating the Effects of Hydrogen Trapping on Fish-scaling Resistance of Enameled Steels
Analysis and Detection of Road Surface Defects Using Multiple Sensing Methods
Auger Spectroscopy Analysis of Alpha Brass Fracture
Austenite Stability Under Focused Ion Beam Milling
Automated Serial Sectioning as a Method to 3D Map Inclusions in Structural Metals
Autonomous Light Optical Microscopy for Quality Control Screening
Calibrating Yield Criteria in 6 Dimensions: A Collection of Analytic and Experimental Case Studies
Case Study of A36 Steel Plate
Characterization of Corrosion Product Deposits on Fuel Cladding Surface Under Various Heat Flux Conditions
Characterization of Iron Ore Sinter Samples by Automated SEM
Characterization of the World's Finest Gold at LANL
Comparison of Diffraction Techniques for Texture Evaluation in Triaminotrinitrobenzene (TATB)
Compressive Response of Ice-templated Ceramic-polymer Composites in Relation to Composition, Microstructure and Loading Orientation
Connecting Dynamic Strain Aging to Deformation Processing in Magnesium-calcium-based Alloys
Correlative Microscopy Studies of Dislocations in a Hot-roll AZ31 Mg Alloy
Deformation Behavior of Hexagonal Metals Investigated by the In-situ Acoustic Emission and Digital Image Correlation Techniques
Deformation Behavior of Mg-Al-Mn Sheets
Determining Bulk Elastic Properties of Transversely Isotropic Aluminum Using Resonant Ultrasound Spectroscopy
Dynamic Mechanical Behavior and Microstructure Evolution of Quinary Cu-Mn-Ni-Zn-Al Alloys
EBSD Characterization of Aluminum Magnesium Alloys
Effect of Acidic Attack on the Structural Characteristics of Sepiolite from Nevada, USA
Effect of Dual-phase Stabilization via Varying Ti/Nb Ratios on the Pitting Behavior of AISI 347 Welds
Effect of Microstructure on Cleavage Fracture of Thick Section Quenched and Tempered S690 High Strength Steel
Effect of Pre-Treatment During Leaching of High Iron, Cobalt Containing Ore
Effect of Thermal Aging on Impact Toughness of Electron Beam Welded AISI 316 Stainless Steel
Effects of Cooling Rate and Ti Addition on Microstructure, Mechanical Properties and Corrosion Characteristics of Laser Deposited Ti-6Al-4V Alloy
Epsilon to Tau Phase Transformation in MnAl Alloys
Experimental Research on Pellet Production with Boron-containing Concentrate
Fatigue Resistance of Low Pressure Nitrided Cr-Mo Low Alloy Steels
From Fundamental Research to Engineered Components: Application to 3D Materials Science
Growth and Characterization of Metal Nanowhiskers
In-situ Raman Microprobing and Ex-situ Raman Mapping of Indented Glasses
In-Situ X-ray Tomography of Vapor Phase Alloying of Ni Wires via Pack Titanization
Influence of PWHT on Impact Toughness of Electron Beam Welded AISI 409 Stainless Steel
Influence on the Structural and Magnetic Properties of the Pre-alloyed Gas-atomized Maraging Steel Powder During Mechanical Milling
Introducing 3D-LIBS, a Powerful Rapid Chemical Mapping Tool for Trace Elements in Complex Materials
Investigation of Impact Toughness of Electron Beam Welded AISI 321 SS at Cryogenic Temperatures
Investigation of Stress Corrosion Crack Initiation Sites in Alloy 600 using 3D EBSD and Local Model
K-100: Investigations on Flotation Separation of Scheelite from Calcite and Fluorite Using ZT as Depressant
K-101: Iron Ore Fines Granulation in a New High-speed Mixing Granulator
K-103: Magnetic and Microstructure Properties of Co-doped Rapidly Solidified Ni50Mn25-xCoxGa25 Heusler Alloys
K-104: Mechanical and Morphological Properties of Hybrid Composites Based on Recycled LDPE/EVA Blend Reinforced with Clay and Babassu Fiber Residues
K-105: Mechanical Behavior of the Multidirectional Natural Hybrid Fabric with Surface Treatment Application Incorporated into the Epoxy Matrix
K-106: Microstructural Characterization of a Metallic Armor
K-107: Microstructural Transformations in a High Hardness Armor Steel, After Ballistic Test with a 7.62 AP
K-108: Observation of Topological Defects in Synthetic Antiferromagnets with Inverted Dzyaloshinskii-moriya Interaction
K-109: Orientation-induced Variability Range in Indentation-measured Elastic Modulus of Molecular Crystals
K-110: PALF Reinforced Epoxy Composite Applied in a Rigid Armor System
K-111: Preparation of Lithium Ion Battery Anode Materials from Precipitation Flotation Product
K-112: Preparation of Vanadium Powder by Thermal Reduction: A Review
K-113: Processing and Characterization of Polyethylene-AgNPs Films – Biocide Effect
K-114: Production and Characterization of PBAT Reinforced with Clay and Graphene Oxide Nanosheets - A Comparative Study
K-115: Reducing and Restoring the Strength of Rocks with Periodic Mechanical Effects
K-118: Simulation and Additive-manufacturing of the Smallest Flute: Design and Fabrication of an Acoustic Sensor to Measure Flow Parameters
K-119: Solder Cup Wire Insertion Study
K-120: Statistical Analysis Applied to Ceramic Pellets Produced with (Al2O3 + Nb2O5 + LiF) at Different Temperatures with Different Watermills
K-122: Study of Styrene Effect on Non-radiation Grafting of Vinyl Benzyl Chloride on to Polyethylene-based Anion Exchange Membrane
K-124: Study on the Effect of Ultraviolet Radiation on Interfacial Resistance between Polyaramide Thermoset Resin
K-125: Study on the Separation of Zinc and Iron in Electric Arc Furnace Baghouse Dusts and Its Kinetics
K-126: Synthesis and Characterization of Batio3 Doped with Eu3+ by the Reaction Solid State Method
K-127: Synthesis and Characterization on Copper Oxide Anode of Lithium-Ion Battery
K-129: The Experimental Study on Combustibility of Semi-coke and Pulverized Coals Injected in Blast Furnace
K-130: Thermal and Mechanical Properties of Iron-actinides Intermetallic Compounds Existed in Metallic Phase of Fuel Debris
K-131: Thermal Behavior of Epoxydic Matrix Composites Reinforced with Graphene Oxide Functionalized Curauá Fibers
K-132: Thermal Characterization of Human Hair
K-135: Weibull Analysis of Tensile Strength of High-performance Epoxy Matrix Composites Reinforced with Curaua Natural Fibers
K-136: Wettability of Liquid Phase Caesium Compounds against Metal Oxides Including UO2 and ThO2
K-34 (Invited): Ballistic Tests in Multilayered Armor Systems Using Natural Lignicellulosic Fibers Reinforced Polymer Composites
K-35: A Comparison between Graphene Oxide and Reduced Graphene Oxide as Reinforcement Agents in Polypropylene Nanocomposite Using Irradiated Polypropylene as Compatibilizer
K-36: A New Method to Obtain Cellulose Nanofiber from Wood
K-37: Aluminum Foam as Promising Materials for Ballistic Protection Application
K-39: Analysis of ß´ (Cu4Ti) Precipitation during Isothermal Aging of a Cu-4wt.%Ti Alloy
K-40: Analysis of The Effect of Marine Salinity in Durability of Red Ceramics Calcinated In Different Temperatures
K-41: Analysis of The Elasto-Plastic Behavior of Structural Steels Subjected to Cyclic Loads
K-42: Analysis of the Performance of Applied Tire Residues in Concrete Pavements
K-43: Application of Nanoparticles of ZnO and ZnO-doped-Ag in Polymeric Blend of HMSPP/SEBS for Biocide Activity
K-44: Ballistic Behavior of Walnut Shell Composite
K-45: Ballistic Evaluation of Reinforced Composites with Mauve / Jute Hybrid Fabric for Ballistic Armor
K-46: Ballistic Test of Multilayered Armor with Intermediate Polyester Composite Reinforced with High Concentration of Fique Fabric
K-50: Characterization of a Brazilian Kaolin for Its Use in the Controlled Release of Isoniazid
K-51: Characterization of Bentonite Beneficiation Residue for Use in Structural Ceramics
K-52: Characterization of Clay Mix with Incorporation of Granite Waste to Produce Ceramic Tiles
K-53: Characterization of Composites formed by Low Density Polyethylene (LDPE) and Natural Bamboo Fibers, by Differential Exploration Calorimetry (DSC), Tensile Strength, and Hardness
K-54: Characterization of Hydrogels for Release of Cosmetic Assets Containing Nanoemulsions of Mandellic Acid in Different Concentrations of Pseudoboehmite
K-55: Characterization of STP Effects on Encapsulation Process and How to Attenuate it to Produce PLA, PLA/MMT.K and PLA/O-MMT.K Microcapsules
K-56: Izod Impact Test of Epoxy Composites Reinforced with Arapaima Scales
K-57: Chemical and Mineralogical Characterization of a Cuprite-myargyrite Ore and Proposal of Elimination of Semimetals by Alkaline Bath
K-58: Chemical Characterization and Mineralogical Analysis of Mining-metallurgical Tailing from the State of Morelos
K-60: Crystallization Kinetics and Mechanical Porperties of Zr-Cu-Al-Sm Metallic Glasses and Their Nanocomposites
K-61: Determinations of Trace and Ultra-trace Level Contaminants in Advanced Materials Using Electrothermal Vaporization ICP–OES
K-62: Development and Characterization of a Luminescent Coating for Asphalt Pavements
K-63: Development and Characterization of CoCrCuFeNi(TiAl) High Entropy Alloys
K-64: Development of Non-equiatomic High Entropy Alloys for High Temperature Applications
K-65: Effect of Alloying Elements on Age Hardening and Coarsening of Beta Precipitates in Isothermally Aged Fe-Ni-Al Based Alloys
K-66: Effect of Antioxidant on Resistance to Ammonia Erosion of Carbon Sleeve in Continuous Annealing Furnace for Low Temperature Grain-oriented Silicon Steel Production
K-67: Effect of Different Ti-Sn Intermetallic Compounds Addition on Synthesis of Ti2SnC by Self-propagating High-temperature Combustion Technique
K-69: Dynamic Mechanical Behaviour of Lean Duplex Stainless Steel 2101
K-70: Evaluation of Energy Absorption of the Epoxy Matrix Composite Reinforced with Tucum Fiber Through Izod Impact Test and Ballistic Impact of Ammunition .22
K-71: Evaluation of Shock Impedance of Multilayered Armor Systems with Epoxy Composite Reinforced with Fique Fabric
K-73: Capillary Absorption Evaluation of Different Mortars Applied in Civil Construction
K-74: Evaluation of the Impedance of Shock of Multilayer Armoring with Epoxy Matrix Composite Reinforced with Fibers of Mallow and Hybrid Fabric of Jute and Mallow
K-75: Evaluation of the Mechanical Behavior of Polymeric Composites Reinforced with Oil Palm Fibers
K-76: Evaluation of the Morphological, Thermal and Mechanical Properties of the Epoxy Composite Reinforced with Brazil Nut Shell
K-77: Evaluation on the Design of Guaruman Fiber Reinforcement Epoxy Matrix Composite for Ballistic Application
K-78: Experimental Validation of Molecular Dynamics Simulation Results of Copper Single Crystal in Oriented Torsion
K-79: Fique Fabric with Surface Reinforcements Produced from Natural Graphite
K-80: Functionalization of Curauá Fibers with Graphene Oxide
K-81: Functionalization of Piassava Fibers with Graphene Oxide
K-82: Fundamental Study on Wettability of Pure Metal by Liquid Sodium
K-83: Graphene Oxide Functionalization in Curaua Fiber/Epoxy Composites: Toward Tensile Properties
K-84: High Strain Rate Nanoindentation of Single Crystalline Metals
K-85: How Small Molecules Can Trigger the One-way Effect in Shape Memory Polymers
K-87: Improvement Properties of Polypropylene by Graphene Oxide Incorporation
K-88: Incorporation of Coke Dust Gas (FGD) in Reds Ceramics
K-89: Incorporation of the Light Green Clay into Textile Polyamide Residues Properties
K-90: Influence of Adiabatic Shear Bands on the Ballistic Resistance of High Hardness Armor Steel
K-91: Influence of Pmma Chemical Degradation in Ethanol
K-92: Influence of Sealing Mortar in the Strength of Compression of the Structural Masonry Ceramic
K-93: Influence of the Reduced Graphene Oxide Incorporation on Properties of Acrylonitrile Butadiene Styrene (ABS)
K-94: Influence of UV Radiation in a Composite of Epoxidic Matrix Reinforced with Hybrid Fabric of Mallow/jute
K-95: Influence of UV Radiation in The Ballistic Behavior of a Composite of Epoxydic Matrix Reinforced with Hybrid Mallow/Jute Fabric
K-96: Inhibition of Flame Propagation in Nanocomposites with Expanded Polystyrene Recycled, Clay, Gypsum and Titanium Dioxide
K-97: In-situ Annealing and Orientation Mapping Studies of Deformed Multiphase Materials
K-98: Investigating the Effect of Sintering Temperature on Structural and Tribological Properties of a Nanostructured Ti–20Nb–13Zr Alloy for Biomedical Applications
K-99: Investigation on Mechanical and Thermal Behaviors of PBAT/PLA Blend Reinforced with Reduced Graphene Oxide Nanosheets
Kinetics of Coke Gasification Reaction Catalyzed by Alkali Carbonates
Leaching of Copper, Cobalt and Nickel from Complex Ore
Mapping Grain Morphology and Orientations by Laboratory Diffraction Contrast Tomography
Measuring the Thermal Conductivity of Molten Salts Using a Frequency-domain Hot-wire Technique
Mechanical Behavior of Thermoplastic Filaments Fabricated with the Fused Modeling Deposition Technique
Micromechanical Properties of Marginal Glass Forming Alloys
Microstructural Evolution of γ'-Ni3Al Precipitates Affecting Mechanical Properties of Nickel-based Superalloys
Microstructure Dependent Thermal Conductivity Measurement of Zircaloy-4 Using an Extended Raman Thermometry Method
Microstructure Evolution During Tensile Deformation of Polycrystalline Cobalt
Microstructure Evolution of Additively Manufactured TiC Reinforced Graded Metal Matrix Composite
Modeling and Characterization of Reflection, Absorption, and Scattering in Polycrystalline Materials
Modeling the Anisotropic Mechanical Properties of Fused Deposition Modeling ABS using an Artificial Neural Network - Part 2
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Non-isothermal Reduction Kinetics of Roasted High Alumina Iron Ore Pellets
On the Depth Resolution of Transmission Kikuchi Diffraction (TKD) Analysis
Optical Characterization of Grain Orientation by Directional Reflectance Microscopy
Particle Size Effects on Mechanical Properties of Polymer Bonded Composites for Non-hazardous High Explosive Surrogates
Phase Diagram of In-P Binary System
Phase Transformation Characterization by Means of High Temperature Digital Image Correlation for Graded Thermo-mechanical Processing of Steel Sheet Parts
Pore Network Modelling Analysis of 3D SEM Images of Nano-porous Gold
Preparation and Characterization of Modified Polymer Fibers Membrane with β-cyclodextrin and its Adsorption Properties
Quasi-plastic Zone Characterization of Regular and Si-doped Boron Carbide
Structural and Magnetic Characterization of Magnetic Nanostructures in C2V Thin Films Exhibiting the Anisotropic Dzyaloshinskii-Moriya Interaction
Study on the Influence of Limestone and Hydrated Lime on Pelletizing
Synchrotron X-ray Diffraction and Computed Tomography Studies of Ultrasonic Welding Dissimilar Mg-Fe Metals
Synthesis and Characterization of Ultra-hard Ceramic AlMgB14-based Materials Obtained from AlxMgy Intermetallic Powder and Boron Powder by the Spark Plasma Sintering
Temperature Dependence of Elastic Properties of Beryllium
Temperature, Pressure, and Current Effects on Densification and Mechanical Properties of Nano-grained FeNiZr Consolidated via the Field Assisted Sintering Technology
Tensile Characterization of Austempered Ductile Iron in Aquatic and Gaseous Environments
The Effect of Radiation Damage and Radiolysis on the Corrosion of SiC with and without Corrosion-mitigation Coatings
The Influence Irradiation Conditions on the Microstructural Evolution of Irradiated U-Mo Fuels
The Influence of Microstructure in Stress Relaxation Cracking
Three-Dimensional Characterization of Microstructure and Elemental Segregation of Thermal Spray Coatings
Unconventional Sodium Chloride in Graphene Liquid Cell
Unloading Analysis for Indentation Fracture in Molecular Crystals
Using Convolutional Neural Networks to Visualize Large Serial Sectioning Datasets
Using the New Rotation Vector Base Line Electron Back Scatter Diffraction (RVB-EBSD) Method to Characterize Single Crystal Cast Microstructures
Using Thermo-Calc Software to Produce the Phase Diagram of Zn-Te System
In-situ Investigation of Thermal Characteristics of Novel Flash Processing Technique for Production of Advanced High Strength Steel (AHSS)

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