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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium Powder Materials Processing and Fundamental Understanding
Presentation Title Tunable High-Energy Milling Toolsets for Refractory Nanocrystalline Alloys
Author(s) Colton A. Gilleland, B. Chad Hornbuckle, Kris Darling, Gregory B. Thompson
On-Site Speaker (Planned) Colton A. Gilleland
Abstract Scope The continuous impact of ball bearings with different powders provides a means to drive materials into solid solution while creating a nanocrystalline structure. Key considerations to this processing include the size and hardness of the media, shape and hardness of the milling vessel, and total volume of powder material. While refractory powders often require media and tooling for effective processing, we demonstrate that proper heat treatments of a jacketed tool steel milling vessel can achieve desired mixing as well as nano-crystallite sizes. Using W-10Cr, we link these processing variables to the tooling itself, processing parameters, and even impurity pick-up. These outcomes are then assessed to the nanophase sintering characteristics and mechanical properties in the consolidated billet.
Proceedings Inclusion? Planned:
Keywords Powder Materials, High-Temperature Materials, Process Technology

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Comparative Study on the Direct Energy Deposition Processability of Ti-Nb-Fe Alloys using Two Different Approaches
A Multiscale Thermomechanical Model for Simulating Sintering Distortions in 3D Printed Parts with Internal Lattice Structures
A Novel Method for Reconditioning Reused Laser Powder Bed Fusion Alloy Powder
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Analysis of Defects and Testing of Tungsten Heavy Alloys
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Boosting Mechanical and Tribological Properties in Multi-Walled Carbon Nanotube Reinforced Inconel 718 Fabricated by High-Energy Ball Milling and Spark Plasma Sintering
Bulk Manufacturing of Metal Core Oxide Shell (MCOS) Nano-Capsules Using Iron Nanopowders
Characterization of Machined Hole Surfaces Integrity in Selective Laser Melted Ti–5Al–5Mo–5V–3Cr Alloy
Characterization of Titanium Hydride Powders: Laser-Induced Breakdown Spectroscopy (LIBS) and Quartz-Crystal Microbalance (QCM) Methods for In-Situ Hydrogen Quantification
Comparison of DED Nozzles’ Performance via In Situ Synchrotron Radiography
Controlling Embrittlement in Refractory Nanophase Separation Sintering Alloys
DEM Modeling of Spherical Particles to Improve Packing Density and Debind Performance in Sinter-Based Additive Manufacturing Processes
Developing PM High Entropy Alloys to be Used in Extreme Conditions: High Temperature, Corrosion and Hydrogen Embrittlement
Development and Optimization of a Nanoscale ZrO2 Suspension for Ceramic Stereolithography: Investigating Rheological Properties and Printing Parameters.
Development of Functionally Graded Al Metal Matrix Layered Hybrid Composite Reinforced with CNT ,Y2O3 & SiC Through PM Route
Dimensional and Geometrical Changes During Sintering of Binder Jetted Components
Direct Vat Photopolymerisation of Hierarchically Porous SiC Loaded With Co/Ni Based Catalysts by Utilising Pickering Emulsions
Effect of Vacuum Heat Treatment on the Oxygen Concentration And Microstructural Features of 316H Stainless Steel Powder for PM-HIP
Effects of Powder Morphology and Capillary Phenomena in Liquid Phase Sintering of Binder Jet Additively Fabricated WC-Co Composite
Enabling the Manufacturing of Hierarchical and Layered Materials
Engineering of Ceramic Oxides Microstructures using Low Temperature Sintering Processes
Enhancing Aluminum with Graphene: Advances in Resistance-Based Sintering for High Conductivity Composites
Enhancing Performance of Aluminium Metal Matrix Composites through Customized Reinforcement Distribution in Multi-Scale Segregated Structures
Evaluating the Antibacterial Efficacy of Copper Alloys with Variable Alloying Element Concentrations: An Empirical Study
Evaluation of Effect of Particle Shape on Sintering Behavior by Large-Scale Phase-Field Simulations
Experimentally and Computationally Driven High-Throughput Materials by Design
Exploring Sintering Behavior of High-Entropy Alloy Nanoparticles (HEA-NPs)
Fabrication of Iron Powder and Adjustment of Particle Size by Rotary Cup Atomizer-Water Curtain Process
Fabrication of Ti6Al4V Spherical Powders for Additive Manufacturing from Recycled Shavings
High Intensity Electric Nano Pulsing Technology for Rapid Materials Processing and Sintering
Impurity Analysis of Powder from Different Material Systems Synthesized via Vacuum-Induction-Melting and Ultrasonic Atomization Powder
Influence of Heat Treatments on Ni-Based Superalloy Densified by Spark Plasma Sintering : Evolution of PPBs and Grain Boundaries Overlap
Influence of Manufacturing Processes on the Microstructure and Properties of High-Entropy Alloys for Advanced Applications
Integrating Molecular Dynamics and Experimental Techniques to Study Flash Sintering of Zirconia and 8% YSZ
Interface Structure and Characteristics of High Temperature Carbide Ceramics Co-Sintered with Lightweight Carbon-Carbon Composites
Investigating the Stability and Electronic Structure of Chromium Copper Oxide Catalysts Using XPS and DFT Modeling
Large Scale DEM Simulations and Computational Performance Evaluation
Low Energy Densification Processes for Ceramic Powders: Processing to Properties
Mechano-Chemical Competition in Mechanically Driven Complex Concentrated Alloys
Metallurgical Evaluation of Near-Canister Degradation of Charpy Toughness Observed in Low Alloy Steel Billets Produced by PM-HIP
Microstructural and Mechanical Properties of 6061 Aluminum Alloy Produced Through the Bound-Metal FFF Additive Manufacturing Process
Microstructural Evolution of Aluminum Alloy Powders Through In-Situ TEM and DICTRA Simulations
Moving Towards the Eco-Design of Flexible Piezoelectric Energy Harversters: Some Issues and Prospects
Multi-Step Mechanical Milling of Metal Swarf into Additive Manufacturing Feedstock Powder
Net Shape Hydroxyapatite Components via 3D-Printing and Sintering
Optimization on Yield Production of Nanoporous Copper Powders via Chemical Dealloying
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Pm-HIP Production of Ductile Tungsten
Powder Alloys for Green Body Printing and Sintering
Powder Flowability of Elemental Niobium, C103, and Other Structural Materials for Powder Bed Fusion
Processing of Barium Zirconate-Based Protonic Conductors by Suitable Combination of Cold Sintering and Post Thermal Treatment
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Progress on Thermal Sprayed Ultrahard Coatings for Preventing Adhesive Wear of Stamping Die Surfaces
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Sustainable Fe/FexOy for SMCs: Effects of Fe Powder Feedstock, Morphology and Particle Size
Sustainable Reconditioning of Stainless-Steel Powder via Disk Milling
Temperature Sensitive Isotropic Sintering Model for 316L Binder Jetting Parts
The Fabrication of TiAl Composited with Near α-Ti Alloys using SPS and HIP
Thermal and Mechanical Property of Cu Material Composites as a Function of Ti and Cr Content by a Spark Plasma Sintering (SPS)
Thermodynamic Analysis of Fe-Al-Si Powder Prepared from Steel Slag by Molten Salt Electrolytic
Tunable High-Energy Milling Toolsets for Refractory Nanocrystalline Alloys
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