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Meeting MS&T24: Materials Science & Technology
Symposium Additive Manufacturing of Ceramic-based Materials: Process Development, Materials, Process Optimization and Applications
Presentation Title Rapid Volumetric Microwave Curing of Silicon Nitride Ceramic Binder Mixtures
Author(s) Saptarshi Mukherjee, Ethan Rosenberg, Johanna Vandenbrande, Johanna Schwartz, Maxim Shusteff, Joseph W. Tringe, James Kelly
On-Site Speaker (Planned) Saptarshi Mukherjee
Abstract Scope Advanced manufacturing methods for ceramics rely on a layer-by-layer construction that are time consuming and costly. Recent development of an optical volumetric additive manufacturing (VAM) technology has enabled rapid 3D printing in a singular step. However, optical VAM is limited to transparent photo resins. Here we propose to develop a fast, scalable VAM system for ceramic materials utilizing microwave radiation. The concept relies on developing a high-power microwave antenna array coupled to a beamforming algorithm to superimpose multiple microwave beams and deliver localized energy to arbitrary 3-D volumes. While current stereolithography techniques require large polymer binder volumes (>50 vol.%) that can lead to sub-surface voids after post-processing and long processing times, we discuss microwave sensitive polymer formulations that can be used in low volume fractions (<40 vol.%) to control microwave energy and achieve rapid, focused green body curing. Results from preliminary experiments on Silicon Nitride ceramic mixtures will be presented.

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

Dense Complex Shape Ceramic Components Fabricated By Digital Light Printing (DLP) and Liquid Silicon Infiltration (LSI)
Densification and Microstructure Evolution of Alumina Structures via Direct Ink Writing
Density Improvement of Binder Jet Printed MnZn Ferrite Cores via Pre-and Post- Sintering Improvement Strategies
Direct Ink Writing of SiOC Structure from Preceramic Polymer Containing Inactive Fillers
Dispersion of PMN-PZT for Direct Ink Writing
Fused Filament Fabrication of Ceramic Matrix Composite Preforms Via Thermo-Oxidative Stabilization of Polyetheretherketone
Interface Stability of Iron-Carbide Materials Fabricated via Laser-Direct Energy Deposition
Irradiative Ceramization of Chemically Bound Phosphate Ceramics (CBPCs) to Enable Direct Additive Manufacturing of Ceramic Composites
Laser-Directed Energy Deposition Additive Manufacturing of Lunar Highlands Simulant (LHS-1) Lunar Regolith Simulant for In Situ Resource Utilization
Multi Ceramic Additive Manufacturing Based on Novel Digital Light Processing Technology
Optimizing SiC Slurries for Robocasting High-Performance SiC.
Rapid Volumetric Microwave Curing of Silicon Nitride Ceramic Binder Mixtures
Stabilization of Alumina Dispersed Slurry by Controlling pH
Towards Direct Additive Manufacturing of Bulk Ceramics Using Selective Laser Flash Sintering
Use of 2D Ti3C2 MXene as an Additive in SiC and Their High-Temperature Phase Behavior
Using Laser Ultrasonics to Correlate Young’s Modulus to Particle Neck Size in Early-Stage Sintering

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