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Meeting 2025 TMS Annual Meeting & Exhibition
Symposium REWAS 2025: Sustainable End-of-Life Management and Recycling Solutions for Batteries, Wind Turbines, and Photovoltaics
Presentation Title D-46: A Preliminary Study on the Recycling of Oxide-Based Solid-State Electrolytes
Author(s) Hyunjoon Lee, Hyunju Lee, Mooki Bae, Jongwon Choi, Sookyung Kim
On-Site Speaker (Planned) Hyunjoon Lee
Abstract Scope Currently, lithium secondary batteries are representative eco-friendly energy around the world, but they have problems with low stability such as explosion and ignition. As All-solid state batteries are being discussed as promising next-generation secondary batteries to solve this problem, leading recycling studies are also considered necessary. All-solid-state batteries are classified according to the composition and structure of the solid electrolyte, and a high share of oxide-based and sulfide-based solid-state electrolytes is expected in the future. In the case of sulfide-based solid electrolytes, it is difficult to recycle through hydrometallurgy due to their high reactivity with moisture, so LLZO (Li7La3Zr2O12) in oxide-based solid-sate electrolytes was separated using a selective precipitation method through this study, and each was separated through the addition of oxalic acid, Na3PO4 and pH control. It was confirmed that co-precipitation did not occur in each reaction, and the recovery rates of all elements were 90% or more.
Proceedings Inclusion? Planned:
Keywords Hydrometallurgy, Recycling and Secondary Recovery, Ceramics

OTHER PAPERS PLANNED FOR THIS SYMPOSIUM

A Separation-Free and Purification-Free Method for Direct Production of Lithium-Rich Solution from Industrial-Grade Lithium-Ion Battery Waste
Advancing Circular Economy: Copper Recovery from E-Waste at Aurubis' New US Facility
Barriers and Opportunities for Recycling Wind Turbine Blades in the United States
D-46: A Preliminary Study on the Recycling of Oxide-Based Solid-State Electrolytes
D-47: Assessing Circular Economy in Photovoltaics: Life Cycle Perspective of Material Recovery, Reuse, and Remanufacturing
D-48: Enhancing Graphite Flotation Efficiency in the Presence of PVDF Binder via Surface Modifications by Ultrasound and UV Irradiation
D-49: Pilot-Scale Hydrometallurgical Recycling of NMC Blackmass
D-50: Solubilities of Lithium, Nickel, and Cobalt Oxides in Deep Eutectic Solvents
D-51: Solvo-Metallurgical Process for the Extraction of Lithium from End-of-Life Electric Vehicle Lithium-Ion Batteries
D-52: Supply Risk Aware Alloy Discovery and Design
Decommissioning, Characterization and Proposed Recycling Route of a Used Na-ZnCl2 Battery Cell
End-of-Life Recycling of Lithium-Ion Batteries in India
Evaluating the Use of Wind Blade Residue and Recycled Aggregate in Low-Strength Concrete
Formation and Stability of Hydrides During Hydrogenation of NdFeB Magnets
Leaching Studies of LiCoO2 Cathode Powder in Phosphoric Acid Medium
Opportunities and Challenges in Lithium-Ion Battery Recycling: Emphasis on Pretreatment and Pyrometallurgical Processing
Optimizing Early-Stage Lithium Recovery: Investigating Oxalic Acid Leaching of Black Mass from End-of-Life NMC 622 Batteries
Photovoltaic Waste Management: Technologies and Strategies to Recycle c-Si and CI(G)S PV Waste
Re-Use of Wind Turbine Blades as Pedestrian Bridges in Beaverbrook Park
Recycling of Lithium-Ion Batteries Cathode Material Using Supercritical Fluid Extraction
Recycling of Raw-Crushed Wind-Turbine Blade for Concrete Production: Mechanical and Durability Performance
Recycling of Solar Wafers Through Acid Leaching and Vacuum Refining
Reductive Leaching Investigation of Li-NMC Cathode Material Related to Spent Battery Recycling
Reductive Leaching of Cathode Active Material from Li-Ion Batteries and Recovery of Copper Reductant
Reviews and Perspectives: Selective Leaching—A Promising Approach for Recycling Lithium Iron Phosphate Batteries
Sustainable Route for Nd Recycling from End-of-Life NdFeB Magnet Using a Deep Eutectic Solvent
Synergistic Processing of Mixed LFP-NMC Black Mass for Improved Recycling Operations
Upcycling Spent Battery Cathodes into Steel with Green Hydrogen

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